荧蒽
克丽舍恩
蒽
芘
化学
色谱法
荧光
环境化学
有机化学
物理
量子力学
作者
Jia-Wen Wei,Jia-Rong He,Shiyi Chen,Yongsheng Guo,Xiaohong Huo,Nuan Zheng,Shuo‐Hui Cao,Yao‐Qun Li
出处
期刊:Food Control
[Elsevier]
日期:2024-04-01
卷期号:158: 110205-110205
标识
DOI:10.1016/j.foodcont.2023.110205
摘要
Polycyclic aromatic hydrocarbons (PAHs) are one of the leading causes of human cancer. Four typical PAHs (PAH4) including benzo(a)pyrene (BaP), benzo(b)fluoranthene (BbF), benzo(a)anthracene (BaA), and chrysene (Chr) have been regarded as reasonable indicators for the occurrence of PAHs in food. In this study, the constant wavelength synchronous fluorescence (CWSF) spectra of PAH4 mixtures were used as the data sets without preprocessing and directly combined with the back propagation neural network (BPNN) algorithm to establish a quantitative analysis method of PAH4. This method is capable of predicting the concentrations of PAH4 in edible oil samples without pre-separation. The detection limits for BaP, BbF, BaA, and Chr were 0.014, 0.068, 0.026, and 0.013 μg/kg, respectively. The recoveries in various oil samples for BaP, BbF, BaA, and Chr were 99.5 ± 2.1, 101.0 ± 4.6, 98.6 ± 3.2, and 98.5 ± 4.9 %, respectively. The proposed method has proved to be a powerful tool for the rapid detection of PAH4.
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