Low-Cost Method for Quantifying Sodium in Coconut Water and Seawater for the Undergraduate Analytical Chemistry Laboratory: Flame Test, a Mobile Phone Camera, and Image Processing

海水 背景(考古学) 化学 仪表(计算机编程) 校准 考试(生物学) 分析化学(期刊) 环境科学 环境化学 工艺工程 计算机科学 数学 统计 工程类 生态学 地质学 有机化学 生物 操作系统 古生物学
作者
Edgar P. Moraes,Nilbert S. A. da Silva,Camilo L. M. Morais,Luiz Seixas das Neves,Kássio M. G. Lima
出处
期刊:Journal of Chemical Education [American Chemical Society]
卷期号:91 (11): 1958-1960 被引量:40
标识
DOI:10.1021/ed400797k
摘要

The flame test is a classical analytical method that is often used to teach students how to identify specific metals. However, some universities in developing countries have difficulties acquiring the sophisticated instrumentation needed to demonstrate how to identify and quantify metals. In this context, a method was developed based on the flame test to quantify sodium in coconut water and seawater using recorded videos of a flame during the experiment and subsequent image treatments with an R statistics platform. This experiment provided undergraduate students an opportunity to study important topics such as atomic theory, emission spectroscopy, quantitative analysis, and image processing. Finally, students measured the sodium content in seawater collected from a region of the Rio Grande do Norte coast, an important region for manufacturing salt. They obtained sodium concentrations that ranged from 11.2 to 12.2 g dm–3 and calibration curves that presented good linearity (R2 > 0.91). The sodium content of coconut water determined was 48 ± 4 mg dm–3. The results demonstrate an interesting and simple method that can easily be applied in experimental Analytical Chemistry courses, and this experiment would also be appropriate for pre-college students.
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