纳米复合材料
材料科学
检出限
电化学
生物传感器
纳米技术
电极
线性范围
电化学气体传感器
化学工程
胶体金
纳米颗粒
化学
色谱法
工程类
物理化学
作者
Mesfin Zewdu,Taniya Sandhu,Navjeet Kaur Lotey,Mulualem Abebe,Olu Emmanuel Femi,Priyanka Sabherwal
出处
期刊:Journal of The Electrochemical Society
[The Electrochemical Society]
日期:2023-04-01
卷期号:170 (4): 047513-047513
被引量:1
标识
DOI:10.1149/1945-7111/acca4d
摘要
A simple, two-step AuNPs/rGO-MWCNTs nanocomposite fabrication methodology, via drop-casting of rGO-MWCNTs on bare screen printed electrode (SPE) followed by electrodeposition of AuNPs through voltammetric scanning, without using any toxic reducing agents is reported. Each step of the synthesized nanocomposite is characterized using state-of-art spectroscopic and electrochemical methods. Our results demonstrate that the nanostructured AuNPs/rGO-MWCNTs/SPE showed synergistic effects of high electrocatalytic and electron transfer activity, high surface area to volume ratio, that confirms our synthesized material is the best material to fabricate a portable device for rapid, inexpensive, and sensitive electrochemical biosensors. For validation, the fabricated material subjected to electrochemical sensing of BSA protein. Our AuNPs/rGO-MWCNTs nanocomposite exhibited significant and good linear response over 2.5–12.5 μ g ml −1 BSA concentration range, with sensitivity of 1.723 μ A μ g ml −1 and limit of detection (LOD) 0.23 μ g/ml. This portable sensing system with enhanced performance demonstrates great potential for our synthesized AuNPs/rGO-MWCNs/SPE nanocomposite in application of point of care applications, and offers a universal and reliable platform for in biomarker detection.
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